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研究领域

Organic Chemistry

1H-NMR Studies on Organolithiums and Development of New NOE Methods Neue, auf dem nuklearen Overhauser Effekt (NOE) basierende NMR-Methoden erlauben detaillierte Einsichten in die Lösungsstruktur von Lithiumorganylen und verwandten Verbindungen. "Rotating frame"-Methoden sind frei vom "Nulldurchgangsproblem" des NOE. Die Anwendung auf einen bekannten endo-Komplex zwischen tert-Butylamin und einem Calixaren deckte einen Literaturirrtum auf: es liegt ein exo-Komplex vor. Mittels einer Pulssequenz, die auf "Excitation Sculpting" beruht, konnte die Struktur einer chiralen Organolithiumverbindung aufgeklärt und in Zusammenhang mit der Stereoselktivität gebracht werden.

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Dynamic Phenomena in Self-Complementary {2}-Metallocryptates Probed by Solution 133Cs-NMR. New Insights Into Ion Pairing Processes. X-Ray Structure and Solid State NMR Spectra of a Meandering Species H. Maid, F. W. Heinemann, A. Scheurer, N. Mooren, R. W. Saalfrank and W. Bauer Paper dedicated to Prof. Dr. Dr. h. c. Dieter Seebach on the occasion of his 75th birthday Helv. Chim. Acta 2012, 95, 2429 On the Way to Graphane - Pronounced Fluorescence of Polyhydrogenated Graphene R. A. Schäfer, J. M. Englert, P. Wehrfritz, W. Bauer, F. Hauke, T. Seyller and A. Hirsch Angew. Chem. Int. Ed. 2013, 52, 754 Sulfur Species in Graphene Oxide S. Eigler, C. Dotzer, F. Hof, W. Bauer and A. Hirsch Chem. Eur. J. 2013, 19, 9490 Optically Active Tetra-tertbutyl-P5deltacyclene Epimers: Preparation, Spectroscopy, Dynamic Equilibriums, H/D Exchange, and Transition-Metal Complex Chemistry L. Rohwer, C. Höhn, J. Autschbach, W. Bauer, F. W. Heinemann, S. H. Torrell, I. Keller, T. E. Shubina, J. Steffen and U. Zenneck Chem. Eur. J. 2014, 20, 5708 Fused Perylene-Phthalocyanine-Macrocycles: A New Family of NIR-Dyes with Pronounced Basicity J. Schönamsgruber, H. Maid, W. Bauer and A. Hirsch Chem. Eur. J. 2014, 20, 16979 Carbon Nanodots - Towards a Comprehensive Understanding of their Photoluminescence V. Strauss, J. T. Margraf, C. Dolle, B. Butz, T. Nacken, W. Bauer, W. Peukert, E. Spiecker, T. Clark, D. M. Guldi J. Am. Chem. Soc. 2014, 136, 17308 Preparation of Reference Materials for the Determination of Phosphorous Containing Flame Retardants in Styrene-Based Polymers R. U. Betran, T. Roth, A. Latza, M. Pöhlein, M. Wolf, R. Puchta, C. Placht, H. Maid, W. Bauer and R. van Eldik Anal. Bioanal. Chem. 2015, 407, 3023 Synthesis and Atropisomerism oc Cascaded Tetraphenyporphyrin-[60]Fullerene Hybrids S. Schlundt, W. Bauer and A. Hirsch in preparation Mycosporine-like Amino Acids: Exceptional High Proton Affinities as Studied by DFT-Calculations and NMR R. Puchta, M. Klisch, D.-P. Häder and W. Bauer in preparation Analytical Methods for Mycosporine-Like Amino Acids M. Klisch, P. Richter, R. Puchta, W. Bauer and D.-P. Häder Trends in Biochemisty submitted Unusual Intermediate Formation During Bromine-Lithium Exchange in 2-Chloro-5-bromopyridine P.Pierrat, Y. Fort, P. C. Gros and W. Bauer submitted DFT/NMR-Analysis of Solution Dynamics and 195Pt-NMR Shifts of Methylene-Bridged Platinum Biscarbene Complexes S. Ahrens, W. Bauer and T. Strassner submitted A Heteronuclear NMR Approach to Structure and Dynamics of Organolithiums and Related Compounds Review paper W. Bauer in preparation Molecular Geometry of Tetracycline and Doxycycline in the Crystalline State and in Solution Investigated by X-ray, Raman, IR, and NMR Spectroscopy, and via DFT Calculations C. F. Leypold, M. O. Schmitt, M. Reiher, S. Schneider, F. W. Heinemann, D. Sellmann and W. Bauer in preparation NOE-Based NMR Methods Applied to Organolithiums and Others W. Bauer in preparation Solid State NMR and Calculational Studies on Cyclopentadienyllithium W. Bauer, H. Jiao and P. v. R. Schleyer in preparation Notes on "Trivial" NMR Tasks: the "Meso/d,l" Problem and Accidental Isochrony M. Haubner, W. Bauer and R. W. Saalfrank in preparation The Solvent Hetero-NOE in NMR W. Bauer in preparation Homo- and Heteronuclear Couplings Within a Platinum Biscarbene Complex W. Bauer, S. Ahrens and T. Strassner in preparation Hartmann-Hahn Artifacts in ROE Spectra W. Bauer in preparation

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