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不对称合成和合成药物化学

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Jin-Yu Lai, Xiao-Xin Shi and Li-Xin Dai*,“Reversal of Regiochemistry of Wacker-Type Reactions Oriented by Heteroatoms”, J. Org. Chem., 1992, 57, 3485. Xiao-Xin Shi and Li-Xin Dai*, “Halogenation of Stablized Ester Enolates by Cupric Halides”, J. Org. Chem., 1993, 58, 4596. Jin-Yu Lai, Xiao-Xin Shi, Yan-Shen Gong and Li-Xin Dai*, “Palladium-Catalyzed Synthesis of Optically Active Tetrahydro-1,4-oxazine Derivatives”, J. Org. Chem., 1993, 58, 4775. Steven S. Wang, Xiao-Xin Shi, William S. Powell, Tamara Tieman, Steven J. Feinmark and Joshua Rokach*, “Total Syntheses of Proinflammatory Dihydro-12-KETE Metabolites”, Tetrahedron Lett., 1995, 36, 513. Xiao-Xin Shi, Subhash P. Khanapure and Joshua Rokach*, “Deblocking of Dithioacetals and Oxathioacetals Using Periodic Acid under Mild Nonaqueous Conditions”, Tetrahedron Lett., 1996, 37, 4331. Subhash P. Khanapure, Xiao-Xin Shi, William S. Powell and Joshua Rokach*, “Total Syntheses of a Potent Proinflammatory 5-Oxo-ETE and Its 6,7-Dihydro Biotransformation Product”, J. Org. Chem., 1998, 63, 337. Subhash P. Khanapure, Xiao-Xin Shi, William S. Powell and Joshua Rokach*, “Total Syntheses of Tritiated and Deuterated 5-Oxo-ETE, a Novel Inflammatory Mediator”, J. Org. Chem., 1998, 63, 4098. Xiao-Xin Shi* and Qing-Quan Wu, “Deblocking of Dithianes with Diacetoxyiodobenzene”, Syn. Commun., 2000, 30, 4081. Xiao-Xin Shi*, Qing-Quan Wu and Xia Lu, “A Synthesis of (4S)-2-(acetoxymethyl)- 4-(tert-butyl-diphenylsilyloxy)-2-cycpenten-1-one”, Tetrahedron:Asymmetry, 2002, 13, 461-464. Xiao-Xin Shi*, Wei He, Qing-Quan Wu, Jie Yin, Feng Ni and Xiao-Zhou Jin, “Asymmetric synthesis of (1S,6R,7S,9R)-7,9-bis(tert-butyldiphenylsilyloxy)- 3-oxabicyclo[4,3,0]nonan-2-one”, Tetrahedron:Asymmetry, 2004, 15, 2327-2331. Xiao-Xin Shi*, Jian-Zhong Yao, Li Kang, Chun-Li Shen and Fei Yi, “Asymmetric Syntheses of Both Enantiomers of Amphetamine Hydrochloride via Bakers’ Yeast Reduction of Phenylacetone”, J. Chem. Res., 2004, 10, 681. Zhao-Xia Wang, Xiao-Xin Shi, Guo-Rong Chen*, Zhi-Hua Ren, Lei Luo and Jing Yan, “A new synthesis of α-arbutin via Lewis acid catalyzed selective glycosylation of tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate with hydroquinone”, Carbohydrate Res., 2006, 341, 1945-1947. Minze Zhu, Chuantao Cha, Wei-Ping Deng* and Xiao-Xin Shi*, “A mild and efficient catalyst for the Beckmann rearrangement, BOP-Cl”, Tetrahedron Lett., 2006, 47, 4861-4863. Xiao-Xin Shi*, Feng Ni, Hai-Xia Shang, Ming-Le Yan and Jun-Quan Su, “Racemization of (S)-(+)-10,11-dimethoxyaporphine and (S)-(+)-aporphine: efficient preparations of (R)-(-)-apomorphine and (R)-(-)-aporphine via a recycle process of resolution”, Tetrahedron:Asymmetry, 2006, 17, 2210-2215. Xiao-Xin Shi*, Shi-Ling Liu, Wei Xu, and Yu-Lan Xu, "Highly stereoselective Pictet-Spengler reaction of D-tryptophan methyl ester with piperonal: convenient syntheses of Cialis (Tadalafil), 12a-epi-Cialis and their deuterated analogues", Tetrahedron: Asymmetry, 2008, 19, 435-442. Liang-Deng Nie, Xiao-Xin Shi*, "A novel asymmetric synthesis of oseltamivir phosphate (Tamiflu) from (-)-shikimic acid", Tetrahedron: Asymmetry, 2009, 20, 124-129. Shi-Ling Liu, Xiao-Xin Shi,* Yu-Lan Xu, Wei Xu, Jing Dong, "Asymmetric syntheses of (-)-methyl shikimate and (-)-5a-carba-β-D-gulopyranose from D-Arabinose via Mukaiyama-type intramolecular aldolization", Tetrahedron: Asymmetry, 2009, 20, 78-83. Sen Xiao, Xia Lu, Xiao-Xin Shi*, Yu Sun, Li-Li Liang, Xin-Hong Yu and Jing Dong, "Syntheses of chiral 1,3-disubstituted tetrahydro-β-carbolines via CIAT process: highly stereoselective Pictet-Spengler reaction of D-tryptophan ester hydrochlorides with various aldehydes", Tetrahedron: Asymmetry, 2009, 20, 430-439. Liang-Deng Nie, Xiao-Xin Shi*, Kwang Hyok Ko and Wei-Dong Lu, "A Short and Practical Synthesis of Oseltamivir Phosphate (Tamiflu) from (-)-Shikimic Acid", J. Org. Chem. 2009, 74, 3970-3973. Sen Xiao, Xiao-Xin Shi*, Jing Xing, Jing-Jing Yan, Shi-Ling Liu and Wei-Dong Lu, "Synthesis of tadalafil (Cialis) from L-tryptophane", Tetrahedron: Asymmetry, 2009, 20, 2090-2096. Sen Xiao, Xiao-Xin Shi*, Feng Ni, Jing Xing, Jing-Jing Yan, and Shi-Ling Liu, "An efficient and general method for the stereodivergent syntheses of tadalafil-like tetracyclic compounds", Eur. J. Org. Chem., 2010, 1711-1716. Xiao-Xin Shi*, Chun-Li Shen, Jian-Zhong Yao, Liang-Deng Nie, and Na Quan, "Inversion of secondary chiral alcohols in toluene with the tunable complex of R3N-R'COOH", Tetrahedron: Asymmetry, 2010, 21, 277-284. Sen Xiao, and Xiao-Xin Shi*, "The first highly stereoselective approach to the mitotic kinesin Eg5 inhibitor HR22C16 and its analogues", Tetrahedron: Asymmetry, 2010, 21, 226-231. Jing Dong, Xiao-Xin Shi*, Jing-Jing Yan, Jing Xing, Qiang Zhang, and Sen Xiao, “Efficient and practical one-pot conversions of N-tosyl tetrahydroisoquinolines into isoquinolines and N-tosyl tetrahydro-β-carbolines into β-carbolines via tandem β-elimination and aromatization”, Eur. J. Org. Chem., 2010, 6987-6992. Na Quan, Xiao-Xin Shi*, Liang-Deng Nie, Jing Dong, Rui-Heng Zhu, “A green chemistry method for the regeneration of carbonyl compounds from oximes by using cupric chloride dihydrate as a recoverable promoter for hydrolysis”, Synlett 2011, 1028-1032

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