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KATALYSE UND MEMBRANEN Es liegen umfangreiche Erfahrungen zu vielfältigen katalytischen Reaktionen wie Steamreforming von Methan, Partialoxidation von Methan zu Synthesegas, Aromatisierung und Dimerisierung von Methan, Bildung von Dimethylether und Dimethylcarbonat, oxidative und nicht-oxidative Dehydrierung, aber auch Andrussow- und Ostwaldreaktion vor. Die Erfahrungen auf dem Gebiet der Gastrennmembranen liegen insbesondere bei geträgerten Zeolith-, Metal-Organic-Framework (MOF)- und Covalent-Organic-Framework (COF)-Membranen. Auch scale up-freundliche Mixed Matrix-Membranen mit MOF- oder COF-Nanopartikeln als Füllstoff in einer Polymermatrix werden als Gastrennmembran bearbeitet.

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Fan, H., Wang, H., Peng, M., Meng, H., Mundstock, A., Knebel, A., & Caro, J. (2023). Pore-in-Pore Engineering in a Covalent Organic Framework Membrane for Gas Separation. ACS NANO, 17(8), 7584-7594. https://doi.org/10.1021/acsnano.2c12774 Sun, H., Wang, F., Li, X., Caro, J., Meng, H., Wang, N., & An, Q. F. (2023). Facile Fabrication of a Continuous ZIF-67 Membrane for Efficient Azeotropic Organic Solvent Mixture Separation. Angewandte Chemie - International Edition, 62(15), [e202300262]. https://doi.org/10.1002/anie.202300262, https://doi.org/10.1002/ange.202300262 Buck, F., Bunjaku, O., Caro, J., & Schiestel, T. (2022). High-flux CO2-stable oxygen transport hollow fiber membranes through surface engineering. Journal of the European Ceramic Society, 42(4), 1537-1547. https://doi.org/10.1016/j.jeurceramsoc.2021.11.040 Caro, J., & Voigt, I. (2022). Jürgen Caro zum 70. Chemie-Ingenieur-Technik, 94(1-2), 3. https://doi.org/10.1002/cite.202270102 Ding, L., Zheng, M., Xiao, D., Zhao, Z., Xue, J., Zhang, S., Caro, J., & Wang, H. (2022). Bioinspired Ti3C2Tx MXene-Based Ionic Diode Membrane for High-Efficient Osmotic Energy Conversion. Angewandte Chemie - International Edition, 61(41), [e202206152]. https://doi.org/10.1002/anie.202206152 Kißling, P. A., Lübkemann, F., Mundstock, A., Lohaus, L., Haist, M., Caro, J., & Bigall, N. C. (2022). Is freeze-drying an alternative to solvent exchange for the hydration stop of cementitious suspensions? Cement and concrete research, 159, [106841]. https://doi.org/10.1016/j.cemconres.2022.106841 Knebel, A., & Caro, J. (2022). Metal–organic frameworks and covalent organic frameworks as disruptive membrane materials for energy-efficient gas separation. Nature nanotechnology, 17(9), 911-923. https://doi.org/10.1038/s41565-022-01168-3 Li, W., Li, Y., Caro, J., & Huang, A. (2022). Fabrication of a flexible hydrogen-bonded organic framework based mixed matrix membrane for hydrogen separation. Journal of membrane science, 643, [120021]. https://doi.org/10.1016/j.memsci.2021.120021 Rieck genannt Best, F., Mundstock, A., Kißling, P. A., Richter, H., Hindricks, K. D. J., Huang, A., Behrens, P., & Caro, J. (2022). Boosting Dimethylamine Formation Selectivity in a Membrane Reactor by In Situ Water Removal. Industrial and Engineering Chemistry Research, 61(1), 307-316. https://doi.org/10.1021/acs.iecr.1c04149 Rieck genannt Best, F., Mundstock, A., Richter, H., Kißling, P. A., Hindricks, K. D. J., Huang, A., Behrens, P., & Caro, J. (2022). Controlled methylamine synthesis in a membrane reactor featuring a highly steam selective K+-LTA membrane. Microporous and Mesoporous Materials, 337, [111920]. https://doi.org/10.1016/j.micromeso.2022.111920 Wang, R., Zhou, Y., Zhang, Y., Xue, J., Caro, J., & Wang, H. (2022). Ultrathin Covalent Organic Framework Membranes Prepared by Rapid Electrophoretic Deposition. Advanced materials, 34(44), [2204894]. https://doi.org/10.1002/adma.202204894 Yue, W., Wan, Z., Li, Y., He, X., Caro, J., & Huang, A. (2022). Synthesis of Cu–ZnO–Pt@HZSM-5 catalytic membrane reactor for CO2 hydrogenation to dimethyl ether. Journal of membrane science, 660, [120845]. https://doi.org/10.1016/j.memsci.2022.120845 Buck, F., Feldhoff, A., Caro, J., & Schiestel, T. (2021). Permeation improvement of LCCF hollow fiber membranes by spinning and sintering optimization. Separation and Purification Technology, 259, [118023]. https://doi.org/10.1016/j.seppur.2020.118023 Caro, J. (2021). Diffusion coefficients in nanoporous solids derived from membrane permeation measurements. ADSORPTION, 27, 283-293. https://doi.org/10.1007/s10450-020-00262-z Deng, A., Shen, X., Wan, Z., Li, Y., Pang, S., He, X., Caro, J., & Huang, A. (2021). Elimination of Grain Boundary Defects in Zeolitic Imidazolate Framework ZIF-95 Membrane via Solvent-Free Secondary Growth. Angewandte Chemie - International Edition, 60(48), 25463-25467. https://doi.org/10.1002/anie.202110828, https://doi.org/10.1002/ange.202110828 Deng, J., Lu, Z., Ding, L., Li, Z-K., Wei, Y., Caro, J., & Wang, H. (2021). Fast electrophoretic preparation of large-area two-dimensional titanium carbide membranes for ion sieving. Chemical Engineering Journal, 408, [127806]. https://doi.org/10.1016/j.cej.2020.127806 Fan, H., Peng, M., Strauss, I., Mundstock, A., Meng, H., & Caro, J. (2021). MOF-in-COF molecular sieving membrane for selective hydrogen separation. Nature Communications, 12(1), [38]. https://doi.org/10.1038/s41467-020-20298-7 Finashina, E. D., Avaev, V. I., Tkachenko, O. P., Greish, A. A., Davshan, N. A., Kuperman, A., Caro, J., & Kustov, L. M. (2021). Decalin Ring Opening on Heterogeneous Me/Saponite Nanocatalysts (Me = Rh, Ru, and Ir). Industrial and Engineering Chemistry Research, 60(21), 7802-7815. https://doi.org/10.1021/acs.iecr.1c00538 Guo, H., Liu, J., Li, Y., Caro, J., & Huang, A. (2021). Post-synthetic modification of highly stable UiO-66-NH2 membranes on porous ceramic tubes with enhanced H2 separation. Microporous and Mesoporous Materials, 313, [110823]. https://doi.org/10.1016/j.micromeso.2020.110823 Jia, L., He, G., Zhang, Y., Caro, J., & Jiang, H. (2021). Hydrogen Purification through a Highly Stable Dual-Phase Oxygen-Permeable Membrane. Angewandte Chemie - International Edition, 60(10), 5204-5208. https://doi.org/10.1002/anie.202010184 Koehler, T., Strauss, I., Mundstock, A., Caro, J., & Marlow, F. (2021). Reversible Photoalignment of Azobenzene in the SURMOF HKUST-1. Journal of Physical Chemistry Letters, 12(36), 8903-8908. https://doi.org/10.1021/acs.jpclett.1c02489 Yue, W., Li, Y., Wei, W., Jiang, J., Caro, J., & Huang, A. (2021). Highly Selective CO2 Conversion to Methanol in a Bifunctional Zeolite Catalytic Membrane Reactor. Angewandte Chemie - International Edition, 60(33), 18289-18294. https://doi.org/10.1002/anie.202106277, https://doi.org/10.1002/ange.202106277 Ding, L., Li, L., Liu, Y., Wu, Y., Lu, Z., Deng, J., Wei, Y., Caro, J., & Wang, H. (2020). Effective ion sieving with Ti3C2T x MXene membranes for production of drinking water from seawater. Nature Sustainability, 3, 296-302. https://doi.org/10.1038/s41893-020-0474-0 Ding, L., Xiao, D., Lu, Z., Deng, J., Wei, Y., Caro, J., & Wang, H. (2020). Oppositely Charged Ti3C2Tx MXene Membranes with 2D Nanofluidic Channels for Osmotic Energy Harvesting. Angewandte Chemie - International Edition, 59(22), 8720-8726. https://doi.org/10.1002/anie.201915993, https://doi.org/10.1002/ange.201915993 Fan, H., Peng, M., Strauss, I., Mundstock, A., Meng, H., & Caro, J. (2020). High-Flux Vertically Aligned 2D Covalent Organic Framework Membrane with Enhanced Hydrogen Separation. Journal of the American Chemical Society, 142(15), 6872-6877. https://doi.org/10.1021/jacs.0c00927 Fritzsche, S., Chokbunpiam, T., Caro, J., Hannongbua, S., Janke, W., & Remsungnen, T. (2020). Combined Adsorption and Reaction in the Ternary Mixture N2, N2O4, NO2 on MIL-127 Examined by Computer Simulations. ACS Omega, 5(22), 13023-13033. https://doi.org/10.1021/acsomega.9b04494 Hou, Q., Zhou, S., Wei, Y., Caro, J., & Wang, H. (2020). Balancing the Grain Boundary Structure and the Framework Flexibility through Bimetallic Metal-Organic Framework (MOF) Membranes for Gas Separation. Journal of the American Chemical Society, 142(21), 9582-9586. https://doi.org/10.1021/jacs.0c02181 Javed, A., Strauss, I., Bunzen, H., Caro, J., & Tiemann, M. (2020). Humidity-Mediated Anisotropic Proton Conductivity through the 1D Channels of Co-MOF-74. Nanomaterials, 10(7), 1-9. 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Angewandte Chemie - International Edition, 59(47), 20858-20862. https://doi.org/10.1002/anie.202008260, https://doi.org/10.1002/ange.202008260 Rieck genannt Best, F., Mundstock, A., Dräger, G., Rusch, P., Bigall, N. C., Richter, H., & Caro, J. (2020). Methanol-to-Olefinsin a Membrane Reactor with in situ Steam Removal – The Decisive Role of Coking. CHEMCATCHEM, 12(1), 273-280. https://doi.org/10.1002/cctc.201901222, https://doi.org/10.15488/9169 Rosnes, M. H., Pato-Doldán, B., Johnsen, R. E., Mundstock, A., Caro, J., & Dietzel, P. D. C. (2020). Role of the metal cation in the dehydration of the microporous metal–organic frameworks CPO-27-M. Microporous and Mesoporous Materials, 309, [110503]. https://doi.org/10.1016/j.micromeso.2020.110503 Strauss, I., Chakarova, K., Mundstock, A., Mihaylov, M., Hadjiivanov, K., Guschanski, N., & Caro, J. (2020). UiO-66 and UiO-66-NH2 based sensors: Dielectric and FTIR investigations on the effect of CO2 adsorption. Microporous and Mesoporous Materials, 302, [110227]. https://doi.org/10.1016/j.micromeso.2020.110227 Zhao, Y., Wei, Y., Lyu, L., Hou, Q., Caro, J., & Wang, H. (2020). Flexible Polypropylene-Supported ZIF-8 Membranes for Highly Efficient Propene/Propane Separation. Journal of the American Chemical Society, 142(50), 20915-20919. https://doi.org/10.1021/jacs.0c07481 Zhou, J., Zhou, C., Xu, K., Caro, J., & Huang, A. (2020). Seeding-free synthesis of large tubular zeolite FAU membranes for dewatering of dimethyl carbonate by pervaporation. Microporous and Mesoporous Materials, 292, [109713]. https://doi.org/10.1016/j.micromeso.2019.109713 Chokbunpiam, T., Chanajaree, R., Caro, J., Janke, W., Remsungnen, T., Hannongbua, S., & Fritzsche, S. (2019). Separation of nitrogen dioxide from the gas mixture with nitrogen by use of ZIF materials; computer simulation studies. Computational Materials Science, 168, 246-252. https://doi.org/10.1016/j.commatsci.2019.05.025 Gao, X., Li, Z-K., Xue, J., Qian, Y., Zhang, L-Z., Caro, J., & Wang, H. (2019). Titanium carbide Ti3C2Tx (MXene) enhanced PAN nanofiber membrane for air purification. Journal of membrane science, 586, 162-169. https://doi.org/10.1016/j.memsci.2019.05.058 Gu, J., Fan, H., Li, C., Caro, J., & Meng, H. (2019). Back Cover: Robust Superhydrophobic/Superoleophilic Wrinkled Microspherical MOF@rGO Composites for Efficient Oil–Water Separation (Angew. Chem. Int. Ed. 16/2019). Angewandte Chemie - International Edition, 58(16), 5464-5464. https://doi.org/10.1002/anie.201902736 Gu, J., Fan, H., Li, C., Caro, J., & Meng, H. (2019). Robust Superhydrophobic/Superoleophilic Wrinkled Microspherical MOF@rGO Composites for Efficient Oil–Water Separation. Angewandte Chemie - International Edition, 58(16), 5297-5301. https://doi.org/10.1002/anie.201814487, https://doi.org/10.1002/ange.201814487 Gu, J., Fan, H., Li, C., Caro, J., & Meng, H. (2019). Rücktitelbild: Robust Superhydrophobic/Superoleophilic Wrinkled Microspherical MOF@rGO Composites for Efficient Oil–Water Separation (Angew. Chem. 16/2019). Angewandte Chemie , 131(16), 5518-5518. https://doi.org/10.1002/ange.201902736 Hou, Q., Wu, Y., Zhou, S., Wei, Y., Caro, J., & Wang, H. (2019). Fein-Tuning der Porengröße in versteiften ZIF-8_Cm-Gerüsten durch eine Mixed-Linker-Strategie für verbesserte permeative CO2/CH4-Trennung. Angewandte Chemie , 131(1), 333-337. https://doi.org/10.1002/ange.201811638 Hou, Q., Wu, Y., Zhou, S., Wei, Y., Caro, J., & Wang, H. (2019). Ultra-Tuning of the Aperture Size in Stiffened ZIF-8_Cm Frameworks with Mixed-Linker Strategy for Enhanced CO2/CH4 Separation. Angewandte Chemie - International Edition, 58(1), 327-331. https://doi.org/10.1002/anie.201811638 Jiang, Y., Liu, C., Caro, J., & Huang, A. (2019). A new UiO-66-NH2 based mixed-matrix membranes with high CO2/CH4 separation performance. Microporous and Mesoporous Materials, 274, 203-211. https://doi.org/10.1016/j.micromeso.2018.08.003 Li, Z-K., Liu, Y., Li, L., Wei, Y., Caro, J., & Wang, H. (2019). Ultra-thin titanium carbide (MXene) sheet membranes for high-efficient oil/water emulsions separation. Journal of membrane science, 592, [117361]. https://doi.org/10.1016/j.memsci.2019.117361 Ma, X., Wu, X., Caro, J., & Huang, A. (2019). Polymer Composite Membrane with Penetrating ZIF-7 Sheets Displays High Hydrogen Permselectivity. Angewandte Chemie - International Edition, 58(45), 16156-16160. https://doi.org/10.1002/anie.201911226, https://doi.org/10.1002/ange.201911226 Ma, X., Wu, X., Caro, J., & Huang, A. (2019). Seeding-free synthesis of high-performance MFI zeolite membranes on superhydrophobic supports inspired by “like grows like” principle. Microporous and Mesoporous Materials, 288, [109589]. https://doi.org/10.1016/j.micromeso.2019.109589 Montañez, L. M., Strauß, I., Caro, J., & Osten, H-J. (2019). Impact of border traps in ultrathin metal-organic framework Cu3(BTC)2 based capacitors. Microporous and Mesoporous Materials, 277, 136-141. https://doi.org/10.1016/j.micromeso.2018.10.029 Shi, L., Wang, S., Lu, T., He, Y., Yan, D., Lan, Q., Xie, Z., Wang, H., Li, M-R., Caro, J., & Luo, H. (2019). High CO2-tolerance oxygen permeation dual-phase membranes Ce0.9Pr0.1O2-δ-Pr0.6Sr0.4Fe0.8Al0.2O3-δ. Journal of Alloys and Compounds, 806, 500-509. https://doi.org/10.1016/j.jallcom.2019.07.281 Strauss, I., Mundstock, A., Treger, M., Lange, K., Hwang, S., Chmelik, C., Rusch, P., Bigall, N. C., Pichler, T., Shiozawa, H., & Caro, J. (2019). Metal−Organic Framework Co-MOF-74-Based Host−Guest Composites for Resistive Gas Sensing. ACS Applied Materials and Interfaces, 11(15), 14175-14181. https://doi.org/10.1021/acsami.8b22002 Wang, S., Shi, L., Xie, Z., He, Y., Yan, D., Li, M-R., Caro, J., & Luo, H. (2019). High-flux dual-phase percolation membrane for oxygen separation. Journal of the European Ceramic Society, 39(15), 4882-4890. https://doi.org/10.1016/j.jeurceramsoc.2019.06.039 Bunde, A., Caro, J., Kärger, J., & Vogl, G. (Hrsg.) (2018). Diffusive Spreading in Nature, Technology and Society. (1 Aufl.) Springer International Publishing AG. https://doi.org/10.1007/978-3-319-67798-9 Bunde, A., Caro, J., Kärger, J., & Vogl, G. (2018). What the Book Is Dealing With. in A. Bunde, J. Caro, J. Kärger, & G. Vogl (Hrsg.), Diffusive Spreading in Nature, Technology and Society (1 Aufl., S. 3-9). Springer International Publishing AG. https://doi.org/10.1007/978-3-319-67798-9_1 Caro, J. (2018). Quo Vadis, MOF? 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An azine-linked covalent organic framework ACOF-1 membrane for highly selective CO2/CH4 separation. Journal of Materials Chemistry A, 6(35), 16849-16853. https://doi.org/10.1039/c8ta05641b Fan, H., Gu, J., Meng, H., Knebel, A., & Caro, J. (2018). Back Cover: High-Flux Membranes Based on the Covalent Organic Framework COF-LZU1 for Selective Dye Separation by Nanofiltration (Angew. Chem. Int. Ed. 15/2018). Angewandte Chemie - International Edition, 57(15), 4104-4104. https://doi.org/10.1002/anie.201802276, https://doi.org/10.1002/ange.201802276 Fan, H., Mundstock, A., Feldhoff, A., Knebel, A., Gu, J., Meng, H., & Caro, J. (2018). Covalent Organic Framework-Covalent Organic Framework Bilayer Membranes for Highly Selective Gas Separation. Journal of the American Chemical Society, 140(32), 10094-10098. https://doi.org/10.1021/jacs.8b05136 Fan, H., Gu, J., Meng, H., Knebel, A., & Caro, J. (2018). 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Smart Metal-Organic Frameworks (MOFs): Switching Gas Permeation through MOF Membranes by External Stimuli. Chemical Engineering and Technology, 41(2), 224-234. https://doi.org/10.1002/ceat.201700635 Lange, K., Hördemann, C., Schulz-Ruhtenberg, M., & Caro, J. (2018). Porous Nickel Nano-Foam by Femtosecond Laser Structuring for Supercapacitor Application. ChemElectroChem, 5(23), 3688-3694. https://doi.org/10.1002/celc.201801152 Liang, W., Zhou, H., Caro, J., & Jiang, H. (2018). Methane conversion to syngas and hydrogen in a dual phase Ce0.8Sm0.2O2-Δ-Sr2Fe1.5Mo0.5O5+Δ membrane reactor with improved stability. International Journal of Hydrogen Energy, 43(31), 14478-14485. https://doi.org/10.1016/j.ijhydene.2018.06.008 Liu, C., Jiang, Y., Zhou, C., Caro, J., & Huang, A. (2018). Photo-switchable smart metal-organic framework membranes with tunable and enhanced molecular sieving performance. 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