Facile Preparation of Haggite by Reducing V2O5 in Guaiacol/Methanol Solution,Inorganic Chemistry

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Facile Preparation of Haggite by Reducing V2O5 in Guaiacol/Methanol Solution
Inorganic Chemistry ( IF 4.3 ) Pub Date : 2018-07-20 00:00:00 , DOI: 10.1021/acs.inorgchem.8b00987
Fei Yan ₁ , Yunfei Bai ₁ , Yushuai Sang ₁ , Linhao Yu ₁ , Kai Wu ₁ , Kai Cui ₁ , Zhe Wen ₁ , Fuhang Mai ₁ , Zewei Ma ₁ , Hong Chen ₂ , Yongdan Li _{1,

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Affiliation

Haggite-structured V₄O₆(OH)₄ is prepared via a one-step reduction of V₂O₅ in a mixture of guaiacol and methanol. Guaiacol delays the overreduction of Haggite to V₂O₃. The time window for the stable existence of the Haggite phase is enlarged at low temperature.

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