Practical Method for Preparation of (S)-2-Amino-5,5,5-trifluoropentanoic Acid via Dynamic Kinetic Resolution,ACS Omega

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Practical Method for Preparation of (S)-2-Amino-5,5,5-trifluoropentanoic Acid via Dynamic Kinetic Resolution
ACS Omega ( IF 3.7 ) Pub Date : 2019-07-09 00:00:00 , DOI: 10.1021/acsomega.9b01537
Haibo Mei ₁ , Jianlin Han ₁ , Ryosuke Takeda _{2,

3} , Tsubasa Sakamoto ₂ , Toshio Miwa ₂ , Yutaka Minamitsuji ₂ , Hiroki Moriwaki ₂ , Hidenori Abe ₂ , Vadim A Soloshonok _{3,

4}

Affiliation

This work reports an operationally convenient ∼20 g scale synthesis of (S)-2-amino-5,5,5-trifluoropentanoic acid and its Fmoc-derivative via dynamic kinetic resolution of the corresponding racemate.

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