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Unusual behavior of long-range order parameter in Fe 3 Al superstructure under severe plastic deformation in Bridgman anvils
Journal of Alloys and Compounds ( IF 5.8 ) Pub Date : 2018-05-01 , DOI: 10.1016/j.jallcom.2018.02.124
А.М. Glezer , I.A. Timshin , I.V. Shchetinin , M.V. Gorshenkov , R.V. Sundeev , A.G. Ezhova

Abstract By X-Ray diffraction and transmission electron microscopy methods the evolution of long-range order parameters and morphology of antiphase boundaries in Fe3Al superstructure (DO3 type) under high pressure torsion (HPT) in Bridgman anvils at room temperature have been investigated. It was detected a new phenomenon: the partial restoration at the N ≥ 1 of completely destroyed D03 long-range order under the HPT deformation (N - the number of complete revolutions of the movable anvil). It was shown that the discovered effect is due to the activation of low-temperature dynamic recrystallization under the SPD and, as a result, to occurrence of the mixture of deformation fragments and recrystallized grains. The averaged long-range order parameter for the first coordination sphere is equal to 0.24–0.26 at N ≥ 2. It was estimated that the value of restored parameter of ordering inside the recrystallized grains is approaching the initial one at the N = 2 and corresponds to the partial restoring at the N > 2.

中文翻译:

Bridgman 铁砧严重塑性变形下 Fe 3 Al 上层结构长程有序参数的异常行为

摘要 通过X射线衍射和透射电子显微镜方法,研究了室温下Bridgman砧在高压扭转(HPT)下Fe3Al超结构(DO3型)的长程有序参数和反相边界形态的演变。检测到一个新现象:在HPT变形(N-动砧完整转数)下,完全破坏的D03长程有序在N≥1处部分恢复。结果表明,发现的效应是由于 SPD 下低温动态再结晶的激活,从而导致变形碎片和再结晶晶粒的混合。在 N ≥ 2 时,第一协调球的平均长程有序参数等于 0.24–0.26。
更新日期:2018-05-01
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