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TBSOTf-promoted versatile N-formylation using DMF at room temperature
Tetrahedron Letters ( IF 1.5 ) Pub Date : 2019-04-03 , DOI: 10.1016/j.tetlet.2019.04.010 Masayoshi Sakurai , Rina Kawakami , Nobuhiro Kihara
中文翻译:
TBSOTf在室温下使用DMF促进的通用N甲酰化
更新日期:2019-04-03
Tetrahedron Letters ( IF 1.5 ) Pub Date : 2019-04-03 , DOI: 10.1016/j.tetlet.2019.04.010 Masayoshi Sakurai , Rina Kawakami , Nobuhiro Kihara
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Hydrazides and amines were N-formylated by DMF in the presence of tert-butyldimethylsilyl triflate (TBSOTf) at room temperature, in good to excellent yields.
中文翻译:

TBSOTf在室温下使用DMF促进的通用N甲酰化
在室温下,在三氟甲磺酸叔丁基二甲基甲硅烷基酯(TBSOTf)存在下,通过DMF对酰肼和胺进行N-甲酰化,获得良好或优异的收率。