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An Efficient Synthesis of N,N,N‐Substituted 1,4,7‐Triazacyclononane
European Journal of Organic Chemistry ( IF 2.5 ) Pub Date : 2018-04-10 , DOI: 10.1002/ejoc.201800048 Yong Huang 1 , Yajing Liu 2 , Song Liu 1 , Renbo Wu 1 , Zehui Wu 1
European Journal of Organic Chemistry ( IF 2.5 ) Pub Date : 2018-04-10 , DOI: 10.1002/ejoc.201800048 Yong Huang 1 , Yajing Liu 2 , Song Liu 1 , Renbo Wu 1 , Zehui Wu 1
Affiliation
A series of N,N,N‐substituted 1,4,7‐triazacyclononanes were prepared by adjusting the reaction sequences and conditions of the intermediate 1,4,7‐tribenzyl‐1,4,7‐triazonane‐2,6‐dione reduction with LiAlH4, the removal of benzyl with Pd/C, and alkylation.
中文翻译：
N，N，N取代的1,4,7-三氮杂环壬烷的高效合成
通过调节中间体1,4,7-三苄基-1,4,7-三氮杂-2-2,6-二酮的反应顺序和条件，制备了一系列N，N，N-取代的1,4,7-三氮杂环壬烷用LiAlH 4还原，用Pd / C除去苄基，并烷基化。
更新日期：2018-04-10
中文翻译：
N，N，N取代的1,4,7-三氮杂环壬烷的高效合成
通过调节中间体1,4,7-三苄基-1,4,7-三氮杂-2-2,6-二酮的反应顺序和条件，制备了一系列N，N，N-取代的1,4,7-三氮杂环壬烷用LiAlH 4还原，用Pd / C除去苄基，并烷基化。
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