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A Convenient Synthesis of 2-Arylnaphtho[1,2-d]oxazole Derivatives Promoted by Triethylamine
Chinese Journal of Chemistry ( IF 5.5 ) Pub Date : 13 NOV 2007 , DOI: 10.1002/cjoc.200790315 Hong LI , Kun WEI , Yang‐Jie WU
Chinese Journal of Chemistry ( IF 5.5 ) Pub Date : 13 NOV 2007 , DOI: 10.1002/cjoc.200790315 Hong LI , Kun WEI , Yang‐Jie WU
A variety of 2-arylnaphtho[1,2-d]oxazole derivatives were efficiently synthesized in moderate to high yields by the reaction of aromatic aldehydes with 1-amino-2-naphthol derivatives in the presence of triethylamine in refluxing ethanol in air. Seven new 2-arylnaphtho[1,2-d]oxazole derivatives were obtained and characterized by the spectral data and elemental analysis. In addition, the X-ray crystal structures of 2-[4-(N,N-dimethylamino)phenyl]naphtho[1,2-d] oxzole (3d) and 1,1′-bis(naphtho[1,2-d]oxazol-2-yl)ferrocene (3n) have been determined.
中文翻译:
三乙胺促进的2-芳基萘并[1,2- d ]恶唑衍生物的简便合成
在空气中回流的乙醇中,在三乙胺的存在下,通过芳族醛与1-氨基-2-萘酚衍生物的反应,可以中等至高收率有效地合成各种2-芳基萘[1,2- d ]恶唑衍生物。获得了七个新的2-芳基萘[1,2- d ]恶唑衍生物,并通过光谱数据和元素分析对其进行了表征。另外,2- [4-(N,N-二甲基氨基)苯基]萘并[1,2- d ]恶唑(3d)和1,1'-双(萘并[1,2- ]的X射线晶体结构已经确定了d ]恶唑-2-基)二茂铁(3n)。
更新日期:2017-01-31
中文翻译:
三乙胺促进的2-芳基萘并[1,2- d ]恶唑衍生物的简便合成
在空气中回流的乙醇中,在三乙胺的存在下,通过芳族醛与1-氨基-2-萘酚衍生物的反应,可以中等至高收率有效地合成各种2-芳基萘[1,2- d ]恶唑衍生物。获得了七个新的2-芳基萘[1,2- d ]恶唑衍生物,并通过光谱数据和元素分析对其进行了表征。另外,2- [4-(N,N-二甲基氨基)苯基]萘并[1,2- d ]恶唑(3d)和1,1'-双(萘并[1,2- ]的X射线晶体结构已经确定了d ]恶唑-2-基)二茂铁(3n)。