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The formation of 1,2-propadiene-1,3-dithione (carbon subsulfide) from flash vacuum pyrolysis of 1,2-dithiole-3-thiones
Tetrahedron Letters ( IF 1.5 ) Pub Date : 1 July 1996 , DOI: 10.1016/0040-4039(96)00941-0
Carl Th Pedersen

1,2-Propadiene-1,3-dithione (carbon subsulfide) has been obtained by flash vacuum pyrolysis of alkylthio substituted 1,2-dithiole-3-thiones in the temperature range 800–1000°C. The dithione was isolated and characterized in an argon matrix at 10K.

中文翻译:

1,2-二硫代-3-硫酮的快速真空热解形成1,2-丙二烯-1,3-二硫酮(亚硫化碳)

通过在800-1000°C的温度范围内对烷基硫取代的1,2-二硫代-3-硫酮进行快速真空热解,可得到1,2-丙二烯-1,3-二硫酮(亚硫化碳)。分离出二硫酮,并在10K的氩气基质中进行表征。
更新日期:2017-01-31
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