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Synthesis of 9,9′-Spirobifluorenes and 4,5-Diaza-9,9′-spirobifluorenes and Their Application as Affinity Materials for Quartz Crystal Microbalances
ChemPlusChem ( IF 3.0 ) Pub Date : 2017-05-16 04:25:29 , DOI: 10.1002/cplu.201700105 Caroline Stobe 1 , Isabella Pyka 2 , Alexander Linke 2 , Sarah Müller 1 , Gregor Schnakenburg 3 , Siegfried R. Waldvogel 2 , Arne Lützen 1
ChemPlusChem ( IF 3.0 ) Pub Date : 2017-05-16 04:25:29 , DOI: 10.1002/cplu.201700105 Caroline Stobe 1 , Isabella Pyka 2 , Alexander Linke 2 , Sarah Müller 1 , Gregor Schnakenburg 3 , Siegfried R. Waldvogel 2 , Arne Lützen 1
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Two different classes of aza analogues of 9,9′-spirobifluorenes have been synthesized. These were obtained by either furnishing the spirobifluorene with additional pyridyl moieties or by installing the aza function directly into the spirobifluorene core. These structurally rigid compounds were then evaluated as affinity materials for quartz crystal microbalances and proved to be highly potent for the detection of volatile organic compounds.
中文翻译：
9,9'-螺二芴和4,5-Diaza-9,9'-螺二芴的合成及其作为石英微天平亲和材料的应用
合成了两种不同类型的9,9'-螺双芴的氮杂类似物。这些可以通过为螺二芴提供额外的吡啶基部分或通过将氮杂官能团直接安装到螺二芴核中而获得。然后，将这些结构刚性的化合物评估为石英微天平的亲和材料，并证明对检测挥发性有机化合物具有很高的效力。
更新日期：2017-05-31
中文翻译：
9,9'-螺二芴和4,5-Diaza-9,9'-螺二芴的合成及其作为石英微天平亲和材料的应用
合成了两种不同类型的9,9'-螺双芴的氮杂类似物。这些可以通过为螺二芴提供额外的吡啶基部分或通过将氮杂官能团直接安装到螺二芴核中而获得。然后，将这些结构刚性的化合物评估为石英微天平的亲和材料，并证明对检测挥发性有机化合物具有很高的效力。
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