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Synthesis of (E)-prop-1-ene-1,3-diyldibenzene derivatives via direct decarboxylative coupling of α,β-unsaturated carboxylic acids with benzyl boronic acid pinacol ester
Tetrahedron Letters ( IF 1.5 ) Pub Date : 2017-04-26 , DOI: 10.1016/j.tetlet.2017.04.084 Mingxiang Zhu , Zhenjiang Qiu , Yun Zhang , Hongli Du , Jingya Li , Dapeng Zou , Yangjie Wu , Yusheng Wu
中文翻译:
α,β-不饱和羧酸与苄基硼酸频哪醇酯的直接脱羧偶联合成(E)-丙-1-烯-1,3-二基二苯衍生物
更新日期:2017-04-26
Tetrahedron Letters ( IF 1.5 ) Pub Date : 2017-04-26 , DOI: 10.1016/j.tetlet.2017.04.084 Mingxiang Zhu , Zhenjiang Qiu , Yun Zhang , Hongli Du , Jingya Li , Dapeng Zou , Yangjie Wu , Yusheng Wu
The first copper-catalyzed cross-coupling reaction between benzyl boronic acid pinacol ester and α,β-unsaturated carboxylic acids was described. The ready availability of the starting materials and excellent E selectivity make this protocol a safe and operationally convenient strategy for the efficient synthesis of (E)-prop-1-ene-1,3-diyldibenzene derivatives.
中文翻译:
α,β-不饱和羧酸与苄基硼酸频哪醇酯的直接脱羧偶联合成(E)-丙-1-烯-1,3-二基二苯衍生物
描述了苄基硼酸频哪醇酯与α,β-不饱和羧酸之间的首次铜催化的交叉偶联反应。起始原料的易得性和出色的E选择性使该方案成为有效合成(E)-丙-1-烯-1,3-二基二苯衍生物的安全且操作便捷的策略。