Palladium-Catalyzed Synthesis of Nitrones Via Redox Cross-Coupling of Nitro Compounds and Alcohols,The Journal of Organic Chemistry

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Palladium-Catalyzed Synthesis of Nitrones Via Redox Cross-Coupling of Nitro Compounds and Alcohols
The Journal of Organic Chemistry ( IF 3.3 ) Pub Date : 2024-06-25 , DOI: 10.1021/acs.joc.4c00512
Jian Xing ₁ , Hong-Yu Tang ₁ , Jing-Lin Chen ₁ , Zheng Huang ₁ , Jun-Jie Liang ₁ , Yao-Sheng Quan ₁ , Jian-Gang Mao ₁

Affiliation

A novel methodology for the synthesis of nitrones via palladium-catalyzed redox cross-coupling of nitro compounds and alcohols is established. The protocol is a mild, convenient, ligand-free, and scalable synthesis method that can be compatible with various nitro compounds and alcohols. Nitrone is a significant multifunctional platform synthon which can be synthesized directly and efficiently via this tactic from commercially available and cheap raw materials.

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