Synthesis of 2,5-Diphenyl-2H-[1,2,3]triazole-4-carboxylic Acid Appended Phenylalanine for Thixotropic Metallogelation and Stiffness Manipulation,ChemistrySelect

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Synthesis of 2,5-Diphenyl-2H-[1,2,3]triazole-4-carboxylic Acid Appended Phenylalanine for Thixotropic Metallogelation and Stiffness Manipulation
ChemistrySelect ( IF 1.9 ) Pub Date : 2023-09-19 , DOI: 10.1002/slct.202302771
Sahabaj Mondal ₁ , Mrinmay Baidya ₁ , Debasish Haldar ₁

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2,5-diphenyl-2H-[1,2,3]triazole-4-carboxylic acid was synthesized by sequential C−N bond formation and electro-oxidative N−N coupling under metal-free conditions and coupled with L-Phe to develop the gelator, which form gel at pH 11. However, the storage modulus exhibits 8-fold increase upon adding Ca²⁺.

中文翻译：

用于触变金属胶凝和刚度控制的 2,5-二苯基-2H-[1,2,3]三唑-4-甲酸附加苯丙氨酸的合成

在无金属条件下，通过连续的 CN-N 键形成和电氧化 NN-N 偶联合成了 2,5-二苯基-2H-[1,2,3]三唑-4-甲酸，并与 L-Phe 偶联，开发凝胶剂，在pH 11 下形成凝胶。然而，添加Ca ²⁺后储能模量增加8 倍。

更新日期：2023-09-21

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