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A facile one-pot synthesis of [(COD)Pt(CH3)2]
Applied Organometallic Chemistry ( IF 3.7 ) Pub Date : 6 JAN 2005 , DOI: 10.1002/aoc.842
Fei Wen , Helmut Bönnemann

A novel one-pot synthesis of dimethyl(1,5-cyclooctadiene)platinum(II), i.e. [(COD)Pt(CH3)2] (complex 1), was developed in 92% yield using platinum acetylacetonate, 1,5-cyclooctadiene and trimethylaluminium. Complex 1 was fully characterized by 1H and 13C NMR, mass spectrometry, cell dimensions and elemental analysis. Copyright © 2005 John Wiley & Sons, Ltd.

中文翻译:

一种简便的一锅合成[(COD)Pt(CH 32 ]

使用乙酰丙酮铂1,5以92%的收率开发了一种新颖的一锅合成二甲基(1,5-环辛二烯)铂(II),即[(COD)Pt(CH 32 ](配合物1)。 -环辛二烯和三甲基铝。配合物1通过1 H和13 C NMR,质谱,细胞尺寸和元素分析进行了全面表征。版权所有©2005 John Wiley&Sons,Ltd.
更新日期:2017-01-31
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