Modular Synthesis of a Tridecasaccharide Motif of Bacteroides vulgatus Lipopolysaccharides against Inflammatory Bowel Diseases through an Orthogonal One-Pot Glycosylation Strategy,Angewandte Chemie International Edition

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Modular Synthesis of a Tridecasaccharide Motif of Bacteroides vulgatus Lipopolysaccharides against Inflammatory Bowel Diseases through an Orthogonal One-Pot Glycosylation Strategy
Angewandte Chemie International Edition ( IF 16.1 ) Pub Date : 2023-03-03 , DOI: 10.1002/anie.202301351
Yunqin Zhang ₁ , Leilei Wang ₁ , Qingli Zhou ₁ , Zuoshan Li ₂ , Dan Li ₂ , Caixia Yin ₂ , Xiufang Wang ₂ , Guozhi Xiao ₁

Affiliation

A tridecasaccharide from Bacteroides vulgatus mpk lipopolysaccharides has been synthesized for the first time by a strategy involving orthogonal one-pot glycosylation reactions based on glycosyl ortho-(1-phenylvinyl)benzoates, which precluded issues such as aglycone transfer and the unpleasant odor of thioglycoside-based orthogonal one-pot glycosylation.

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