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Continuous and Electrochemical Synthesis of 2,2’,4,4’,6,6’-Hexanitrostilbene
ChemElectroChem ( IF 3.5 ) Pub Date : 2022-03-31 , DOI: 10.1002/celc.202200118
Jiedong Zou 1 , Jie Deng 1 , Yaqi Qin 1 , Tiancheng Li 1 , Xinli Zhou 1 , Ming Lu 1 , Pengcheng Wang 2
Affiliation  

Explosive Synthesis: A continuous method based on the use of a static mixer combined with electrochemistry was used to prepare 2,2’,4,4’,6,6’-hexanitrostilbene for the first time, and the yield of hexanitrostilbene produced by the continuous process reached 65 %. This method concurrently combines the advantages of a simple reaction process for the one-step synthesis of the target product, easy large-scale continuous production, and high yield.

中文翻译:

2,2',4,4',6,6'-六硝基芪的连续电化学合成

爆炸合成:首次采用静态混合器结合电化学的连续法制备2,2',4,4',6,6'-六硝基芪,六硝基芪的收率由连续过程达到65%。该方法同时结合了目标产物一步合成反应过程简单、易于大规模连续生产、收率高的优点。
更新日期:2022-03-31
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