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Generation and characterization of nanobubbles in ionic liquid for a green extraction of polyphenols from Carya cathayensis Sarg
Food Chemistry ( IF 8.5 ) Pub Date : 2021-08-22 , DOI: 10.1016/j.foodchem.2021.130932
Fatima-Ezzahra Ettoumi 1 , Ruyuan Zhang 1 , Tarun Belwal 1 , Miral Javed 1 , Yanqun Xu 2 , Li Li 1 , Lv Weide 3 , Zisheng Luo 4
Affiliation  

Nanobubbles (NBs) generated-nanojets membrane poration have gained enormous attention. In this study, NBs were fabricated as a novel green approach to assist ionic liquid (IL) [C4C1im][BF4] extraction of polyphenols from Carya cathayensis Sarg. husk. NBs were successfully generated with mean size of 85.47 ± 5 nm, zeta potential of +39 ± 2.24 mV, and concentration of 21.15 ± 0.75 × 108 particles/mL (stable for over 48 h in IL solution). Compared to common solutions extract, IL-NBs extract showed significantly higher (p < 0.05) antioxidant activity and polyphenols yields with a total polyphenol, total flavonoid, and total tannins contents of 85.67 ± 2.05 mg GAE/g DW, 42.44 ± 1.17 mg CE/g DW, and 8.2 ± 0.05 mg TAE/g DW, respectively. The SEM results confirmed that NBs’ nanojets caused morphological destruction of the husk powder. Overall, IL-NBs solution showed better extraction efficiency of polyphenols than other solutions, giving insight into a new “green” nanotechnology-based extraction method.



中文翻译:

用于绿色提取山核桃多酚的离子液体中纳米气泡的产生和表征

Nanobubbles (NBs) 产生的纳米喷射膜穿孔获得了极大的关注。在这项研究中,NBs 被制造为一种新的绿色方法,以辅助离子液体 (IL) [C 4 C 1 im] [BF 4 ] 从山核桃中提取多酚。外壳。NBs 成功生成,平均大小为 85.47 ± 5 nm,zeta 电位为 +39 ± 2.24 mV,浓度为 21.15 ± 0.75 × 10 8颗粒/mL(在 IL 溶液中稳定超过 48 小时)。与普通溶液提取物相比,IL-NBs 提取物显示出显着更高的 ( p < 0.05) 抗氧化活性和多酚产量,总多酚、总黄酮和总单宁含量分别为 85.67 ± 2.05 mg GAE/g DW、42.44 ± 1.17 mg CE/g DW 和 8.2 ± 0.05 mg TAE/g DW . SEM 结果证实 NBs 的纳米射流造成了壳粉的形态破坏。总体而言,IL-NBs 解决方案显示出比其他解决方案更好的多酚提取效率,从而深入了解一种基于“绿色”纳米技术的新提取方法。

更新日期:2021-08-27
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