This review article intends to provide insightful advice for dissolution-dynamic nuclear polarization in the form of a practical handbook. The goal is to aid research groups to effectively perform such experiments in their own laboratories. Previous review articles on this subject have covered a large number of useful topics including instrumentation, experimentation, theory, etc. The topics to be addressed here will include tips for sample preparation and for checking sample health; a checklist to correctly diagnose system faults and perform general maintenance; the necessary mechanical requirements regarding sample dissolution; and aids for accurate, fast and reliable polarization quantification. Herein, the challenges and limitations of each stage of a typical dissolution-dynamic nuclear polarization experiment are presented, with the focus being on how to quickly and simply overcome some of the limitations often encountered in the laboratory.

这篇评论文章旨在以实用手册的形式为溶解动态核极化提供有见地的建议。目标是帮助研究小组在自己的实验室中有效地进行此类实验。以前关于这个主题的评论文章涵盖了大量有用的主题，包括仪器、实验、理论等。这里要讨论的主题将包括样品制备和检查样品健康的技巧；正确诊断系统故障和执行一般维护的清单；关于样品溶解的必要机械要求；并有助于准确、快速和可靠的偏振量化。本文介绍了典型溶解-动态核极化实验每个阶段的挑战和局限性，