A Three‐Step Synthesis of 4H‐Cyclopenta[def]phenanthrene from Pyrene,European Journal of Organic Chemistry

当前位置： X-MOL 学术 › Eur. J. Org. Chem. › 论文详情

Our official English website, www.x-mol.net, welcomes your feedback! (Note: you will need to create a separate account there.)

A Three‐Step Synthesis of 4H‐Cyclopenta[def]phenanthrene from Pyrene
European Journal of Organic Chemistry ( IF 2.5 ) Pub Date : 2021-03-16 , DOI: 10.1002/ejoc.202100190
Alex van der Ham ₁ , Hermen S. Overkleeft ₁ , Dmitri V. Filippov ₁ , Gregory Schneider ₂

Affiliation

CPP is a valuable building block in the production of photoactive materials. A short and economical synthesis route to this material is thus much desired. We here report a three‐step procedure, starting from pyrene, which allows access to this material on a gram scale. Our route is characterized by the use of relatively non‐hazardous materials and fully optimized purification protocols.