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3-(4-Amino-1,2,5-oxadiazol-3-yl)-4-(4-nitro-1,2,5-oxadiazol-3-yl)-1,2,5-oxadiazole
Molbank Pub Date : 2014-05-22 , DOI: 10.3390/m824 Philip Pagoria , Maoxi Zhang , Ana Racoveanu , Alan DeHope , Roman Tsyshevsky , Maija Kuklja
Molbank Pub Date : 2014-05-22 , DOI: 10.3390/m824 Philip Pagoria , Maoxi Zhang , Ana Racoveanu , Alan DeHope , Roman Tsyshevsky , Maija Kuklja
The title compound 3-(4-amino-1,2,5-oxadiazol-3-yl)-4-(4-nitro-1,2,5-oxadiazol-3-yl)-1,2,5-oxadiazole (ANFF-1) was synthesized by: (1) by reaction of 3,4-bis(4-nitro-1,2,5-oxadiazol-3-yl)-1,2,5-oxadiazole (BNFF-1) with gaseous ammonia in toluene and (2) by partial oxidation of 3,4-bis(4-amino-1,2,5-oxadiazol-3-yl)-1,2,5-oxadiazole (BAFF-1) with 35% H2O2 in concentrated H2SO4.
中文翻译:
3-(4-氨基-1,2,5-恶二唑-3-基)-4-(4-硝基-1,2,5-恶二唑-3-基)-1,2,5-恶二唑
标题化合物3-(4-氨基-1,2,5-恶二唑-3-基)-4-(4-硝基-1,2,5-恶二唑-3-基)-1,2,5-恶二唑(ANFF-1)通过以下方式合成:(1)通过3,4-双(4-硝基-1,2,5-恶二唑-3-基)-1,2,5-恶二唑(BNFF-1)的反应用甲苯中的气态氨和(2)将3,4-双(4-氨基-1,2,5-恶二唑-3-基)-1,2,5-恶二唑(BAFF-1)与35浓H2SO4中的%H2O2。
更新日期:2014-05-22
中文翻译:
3-(4-氨基-1,2,5-恶二唑-3-基)-4-(4-硝基-1,2,5-恶二唑-3-基)-1,2,5-恶二唑
标题化合物3-(4-氨基-1,2,5-恶二唑-3-基)-4-(4-硝基-1,2,5-恶二唑-3-基)-1,2,5-恶二唑(ANFF-1)通过以下方式合成:(1)通过3,4-双(4-硝基-1,2,5-恶二唑-3-基)-1,2,5-恶二唑(BNFF-1)的反应用甲苯中的气态氨和(2)将3,4-双(4-氨基-1,2,5-恶二唑-3-基)-1,2,5-恶二唑(BAFF-1)与35浓H2SO4中的%H2O2。