Selective and Scalable Electrosynthesis of 2H‐2‐(Aryl)‐benzo[d]‐1,2,3‐triazoles and Their N‐Oxides by Using Leaded Bronze Cathodes,Chemistry - A European Journal

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Selective and Scalable Electrosynthesis of 2H‐2‐(Aryl)‐benzo[d]‐1,2,3‐triazoles and Their N‐Oxides by Using Leaded Bronze Cathodes
Chemistry - A European Journal ( IF 3.9 ) Pub Date : 2020-04-28 , DOI: 10.1002/chem.202000890
Tom Wirtanen ₁ , Eduardo Rodrigo ₁ , Siegfried R. Waldvogel ₁

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Electroreductive synthesis of 2H‐2‐(phenyl)benzo[d]‐1,2,3‐triazole and its N‐oxide from 2‐nitroazobenzene is portrayed in the cover artwork. The electrolytic conversion can selectively stop on the intermediate or final target compound, controlled by the amount of charge applied. The scalable electrosynthesis is run on the simplest electrochemical setup: constant current is applied between two electrodes in an undivided cell. More information can be found in the Communication by S. R. Waldvogel et al. (DOI: 10.1002/chem.201905874).

中文翻译：

铅青铜电极选择性且可扩展地合成2H-2-（芳基）-苯并[d] -1,2,3-三唑及其氮氧化物

电还原合成的2H- 2-（苯基）苯并[ d ] -1,2,3-三唑并从2-硝基偶氮苯它的N-氧化物在封面图案被描绘。电解转化可以选择性地停止在中间或最终目标化合物上，受所加电荷的量控制。可扩展的电合成是在最简单的电化学装置上进行的：恒定电流在一个未分割的电池中的两个电极之间施加。可以在S. R. Waldvogel等人的《通讯》中找到更多信息。（DOI：10.1002 / chem.201905874）。

更新日期：2020-04-28

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