Combination of X-ray Diffraction and Specific Rotation to Unequivocally Characterize Carvone Semicarbazone Derivatives,Journal of Chemical Education

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Combination of X-ray Diffraction and Specific Rotation to Unequivocally Characterize Carvone Semicarbazone Derivatives
Journal of Chemical Education ( IF 2.5 ) Pub Date : 2020-04-23 , DOI: 10.1021/acs.jchemed.0c00074
John J. Dolhun ₁ , Peter Müller ₂

Affiliation

Single-crystal X-ray structures, melting points, and students’ specific rotation results on carvone semicarbazone derivatives are presented with experimental details. Critical parameters are identified to ensure the success of the experiment. Procedures developed here were tested in a laboratory course, consisting of approximately 70 students over three semesters. This experiment teaches undergraduate students important new instrumental methodology for characterizing a sample, allowing students to gain skills from hands-on experience using modern analytical instrumentation, and analyzing data to achieve a conclusion.

中文翻译：

X射线衍射和比旋光的组合可以明确地表征香芹酮半卡巴zone衍生物

给出了香芹酮半卡巴zone衍生物的单晶X射线结构，熔点和学生的特定旋转结果，并提供了实验细节。确定关键参数以确保实验成功。这里开发的程序在实验室课程中进行了测试，三个学期中约有70名学生组成。该实验向本科生教授重要的新仪器方法，以表征样品，使学生可以使用现代分析仪器从动手实践中获得技能，并分析数据以得出结论。

更新日期：2020-04-23

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