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A Large-Scale Low-Cost Preparation of N-Benzylhydroxylamine Hydrochloride
Synthesis ( IF 2.2 ) Pub Date : 2009-08-14 , DOI: 10.1055/s-0029-1216932 Gilles Dujardin , Thanh Nguyen , Arnaud Martel , Robert Dhal
中文翻译:
大规模低成本制备N-苄基羟胺盐酸盐
更新日期:2009-08-14
Synthesis ( IF 2.2 ) Pub Date : 2009-08-14 , DOI: 10.1055/s-0029-1216932 Gilles Dujardin , Thanh Nguyen , Arnaud Martel , Robert Dhal
A high-yielding, practical two-step procedure for the preparation of N-benzylhydroxylamine starting from dibenzylamine is described. As specified in the detailed protocol, the reaction can be conveniently carried out on a > 0.5 mol laboratory scale.
N-benzylhydroxylamine - N-benzylnitrones - 1,3-dipolar cycloaddition - secondary amine oxidation - nitrone hydrolysis
中文翻译:
大规模低成本制备N-苄基羟胺盐酸盐
描述了一种从二苄基胺开始制备N-苄基羟胺的高产率,实用的两步方法。如详细方案中所述,该反应可以方便地在> 0.5 mol实验室规模下进行。
N-苄基羟胺-N-苄基硝酮-1,3-偶极环加成-仲胺氧化-硝酮水解