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A Large-Scale Low-Cost Preparation of N-Benzylhydroxylamine Hydrochloride
Synthesis ( IF 2.2 ) Pub Date : 2009-08-14 , DOI: 10.1055/s-0029-1216932
Gilles Dujardin , Thanh Nguyen , Arnaud Martel , Robert Dhal

A high-yielding, practical two-step procedure for the preparation of N-benzylhydroxylamine starting from dibenzylamine is described­. As specified in the detailed protocol, the reaction can be conveniently carried out on a > 0.5 mol laboratory scale.

N-benzylhydroxylamine - N-benzylnitrones - 1,3-dipolar cycloaddition - secondary amine oxidation - nitrone hydrolysis



中文翻译:

大规模低成本制备N-苄基羟胺盐酸盐

描述了一种从二苄基胺开始制备N-苄基羟胺的高产率,实用的两步方法。如详细方案中所述,该反应可以方便地在> 0.5 mol实验室规模下进行。

N-羟胺-N-苄基硝酮-1,3-偶极环加成-仲胺氧化-硝酮水解

更新日期:2009-08-14
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