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Controllable Fluorocarbon Chain Elongation: TMSCF2Br-Enabled Trifluorovinylation and Pentafluorocyclopropylation of Aldehydes An Liu, Xianghong Zhang, Feng Zhao, Chuanfa Ni, and Jinbo Hu*J. Am. Chem. Soc. 2024.
Sulfur-based organofluorine reagents for selective fluorination, fluoroalkylation, and fluoroolefination reactions xiu wang, Jinbo Hu*2023 Taylor & Francis Group, LLC
Unusual single electron transfer reactions between alkenes and iodine electrophiles Zhengzhao Lou, Jingyu Hu, Chuanfa Ni, Xiu Wang, Jinbo Hu*Chin. J. Chem. 2024,42, 471-477
Switching from 2-pyridination to difluoromethylation: ligand-enabled nickel-catalyzed reductive difluoromethylation of aryl iodides with difluoromethyl 2-pyridyl sulfone Wei Du, Qinyu Luo, Zhiqiang Wei, Xiu Wang, Chuanfa Ni, Jinbo Hu*Sci China Chem 2023,66, 2785–2790
Copper-Catalyzed Enantioselective Difluoromethylation-Alkynylation of Olefins by Solving the Dilemma between Acidities and Reduction Potentials of Difluoromethylating Agents Zhiqiang Wei, Weiqin Zheng, Xiaolong Wan, and Jinbo Hu*Angew. Chem. Int. Ed. 2023, 62, e202308816
From intramolecular cyclization to intermolecular hydrolysis: TMSCF2Br-enabled carbonylation of aldehydes/ketones and amines to α-hydroxyamides An Liu, Shuo Sun, Qiqiang Xie, Rumin Huang, Taige Kong, Chuanfa Ni and Jinbo Hu *Org. Chem. Front. 2023,10,5343-5351
Enantioselective Nucleophilic Trifluoromethoxylation of Racemic Propargyl Sulfonates Ni Chuanfa, Hu Jinbo*Chin. J. Org. Chem. 2023, 43, 2582-2583
Sulfones Bearing Perfluorinated Pyridine Group: Synthesis and Photocatalytic Reaction with α-(Trifluoromethyl)styrenes Artem G. Savchenko, Mikhail O. Zubkov, Vladimir A. Kokorekin, Jinbo Hu, Alexander D. Dilman*ChemCatChem 2023, 15, e202300505
Pentacoordinate Phosphoranes as Versatile Reagents in Fluoroalkylation Reactions Huanhuan Song, Weihao Li, Xiaoying Wang, Kaiteng Wang, Jingwen Li, Shuai Liu, Pin Gao, Xin-Hua Duan, Jinbo Hu and Mingyou Hu*CCS Chem.2023, Just Publishied.
Transition-Metal-Free Controllable Single and Double Difluoromethylene Formal Insertions into C–H Bonds of Aldehydes with TMSCF2Br An Liu, Chuanfa Ni, Qiqiang Xie, and Jinbo Hu* Angew.Chem.Int.Ed.2022, e202217088
Regioselective Aromatic Perfluoro-tert-butylation Using Perfluoro-tert-butyl Phenyl Sulfone and Arynes Zhiqiang Wei, Lixian Wen, Kaidi Zhu, Qian Wang, Yanchuan Zhao*, and Jinbo Hu* J. Am. Chem. Soc. 2022, 144, 48, 22281–22288
Synthesis of fluoroalkenes via Julia and Julia-Kocienski olefination reactions QinyuLuo, XiuWang, JinboHu* Tetrahedron, 2022, 113, 132694
Palladium-Catalyzed Defluorinative Coupling of Difluoroalkenes and Aryl Boronic Acids for Ketone Synthesis Guangwu Sun, Herui Liu, Xiu Wang, Wenbo Zhang, Wenjun Miao, Qinyu Luo, Bing Gao,* and Jinbo Hu* Angew.Chem.Int.Ed. 2022, e202213646
Reagent-Controlled Highly Stereoselective Difluoromethylation: Efficient Access to Chiral -Difluoromethylamines from Ketimines Qinghe Liu , Taige Kong, Chuanfa Ni and Jinbo Hu* Molecules 2022, 27, 7076.
Visible-Light-Promoted S-Trifluoromethylation of Thiophenols with Trifluoromethyl Phenyl Sulfone Zhiqiang Wei, Zhengzhao Lou, Chuanfa Ni, Wei Zhang, and Jinbo Hu* Chem. Commun. 2022, 58, 10024–10027
Dynamic Kinetic Resolution-Enabled Highly Stereoselective Nucleophilic Fluoroalkylation to Access Chiral β-Fluoro Amines Qinghe Liu, Taige Kong, Chuanfa Ni, and Jinbo Hu* Org. Lett. 2022, 24, 32, 5982–5987
Controllable Single and Double Difluoromethylene Insertions into C-Cu Bonds: Copper-Mediated Tetrafluoroethylation and Hexafluoropropylation of Aryl Iodides with TMSCF2H and TMSCF2Br Xiu Wang, Shitao Pan, Qinyu Luo, Qian Wang, Chuanfa Ni, and Jinbo Hu* J. Am. Chem. Soc.2022, 144, 12202–12211.
Synthesis of Aryl Perfluorocyclopropyl Ethers via [2 + 1] Cyclopropanation Using TMSCF2Br Reagent Ran Liu and Jinbo Hu* Org. Lett. 2022, 24, 3589-3593
Copper-mediated pentafluoroethylation of organoboronates and terminal alkynes with TMSCF3 Pan, Shitao; Xie, Qiqiang; Wang, Xiu; Wang, Qian; Ni, Chuanfa; Hu, Jinbo* Chemical Communications, 2022, 58, 5156-5159.
SulfoxFluor-Enabled Deoxyazidation of Alcohols with NaN3 Guo, Junkai; Wang, Xiu; Ni, Chuanfa; Wan, Xiaolong; Hu, Jinbo* Nature Communications, 2022, 13, e2752.
Modified and Scalable Synthesis of N-Tosyl-4-Chlorobenzenesulfonimidoyl Fluoride (SulfoxFluor): Direct Imidation of Sulfinyl Chlorides with Chloramine-T Trihydrate Liu, Renxiang; Zhou, Xiao-Cong; He, Xin-Yi; Li, Yuan-Qiang;* Zheng, Weiqin; Wang, Xiu; Guo, Junkai; Ni, Chuanfa;* Hu, Jinbo* Org. Process Res. Dev. 2022, 26, 380-386.
Cover Profile: S-(Trifluoromethyl) Benzothioate (TFBT): A KF-Based Reagent for Nucleophilic Trifluoromethylthiolation Meng, Depei; Lyu, Yichong; Ni, Chuanfa; Zhou, Min; Li, Yang; Hu, Jinbo* Chemistry-A European Journal 2022, 28, e202200483.
S-(Trifluoromethyl) Benzothioate (TFBT): A KF-Based Reagent for Nucleophilic Trifluoromethylthiolation Meng, Depei; Lyu, Yichong; Ni, Chuanfa; Zhou, Min; Li, Yang; Hu, Jinbo* Chemistry-A European Journal 2022,28, e202104395.
Difluoromethyl 2-Pyridyl Sulfoximine: A Stereoselective Nucleophilic Reagent for Difluoro(aminosulfinyl)methylation and Difluoro(aminosulfonyl)methylation Liu, Qinghe; Ni, Chuanfa; Wang, Qian; Meng, Depei; Hu, Jinbo* CCS Chem.2022,4,3648–3659
TMSCF2Br-Enabled Fluorination-Aminocarbonylation of Aldehydes: Modular Access to α-Fluoroamides Liu, An; Ni, Chuanfa; Xie, Qiqiang; Hu, Jinbo* Angew. Chem.Int. Ed.2022,61, e202115467.
Photoredox-Catalyzed Ring-Opening Addition Reaction between Benzyl Bromides and Cyclic Ethers Cuiwen Kuang,Chuanfa Ni, Yucheng Gu, Jinbo Hu* Synthesis 2021,54,1272-1286
Water-promoted regio-selective trifluoromethylation of vinyl conjugated diazoacetates Xinxin Han, Xin Liu, Yueyun Bao, Hunahuan Song, Yu-Rou Zhao, Xiaoying Wang,Junjie Zhang, Le Liu, Xin-Hua Duan, Jinbo Hu and Mingyou Hu* Org. Chem. Front., 2022, 9, 204–209
Fluorination Triggers Fluoroalkylation: Nucleophilic Perfluoro-tertbutylation with 1,1-Dibromo-2,2-bis(trifluoromethyl)ethylene (DBBF) and CsF Qian Wang, Quan Tao, Hui Dong, Chuanfa Ni, Xiaoming Xie,* and Jinbo Hu* Angew. Chem. Int. Ed. 2021, 60, 27318 –27323 208.jpg
Difluorocarbene-Induced Ring-Opening Difluoromethylation-Halogenation of Cyclic (Thio)Ethers with TMSCF2X (X = Br, Cl) Zhang, Rongyi; Li, Qigang; Xie, Qiqiang; Ni, Chuanfa*; Hu, Jinbo* Chemistry？A European Journal, 2021, 27, 17773–17779.
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